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Novel organic-inorganic hybrid materials of 3-acryloxypropyl trimethoxysilane and 4,49-(hexafluoroisopropylidene)diphenol were synthesized by non-hydrolytic sol-gel processing. Thick, crack-free films were produced by spin-coating without high volume shrinkage during further treatment of the films. The optical properties of the materials were precisely tailored by adjusting the chemical composition of the materials. The tunability of the refractive index allowed us to fabricate step-indexdoi:10.1039/b715111j fatcat:txzaw5nf4vctrfpc7zr3jl2ei4