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The Mg-Al layered double hydroxides (Mg-Al LDH) film was fabricated on anodized magnesium alloy AZ31 at different reaction temperature by in-situ hydrothermal treatment method. The reaction solution contained only one kind of trivalent cation Al 3+ , and the divalent cation Mg 2+ is provided by the anodic oxide films. The structure, composition and morphology of the Mg-Al LDH films were investigated via XRD, FI-IR and SEM, respectively. The corrosion resistance of films was studied usingdoi:10.20964/2017.07.74 fatcat:aocipajharepva34nhspslpogu