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High-pressure synthesis and crystal structure of the mixed-cation borate Ga4In4B15O33(OH)3
2019
Zeitschrift für Naturforschung. B, A journal of chemical sciences
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The mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4)
doi:10.1515/znb-2019-0014
fatcat:tcp52vniira67lieh6sewtmxve