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Two kinds of nano-structural graphite were prepared from graphite powder by ball-milling under hydrogen or argon atmosphere, where each product is denoted as HG or AG, respectively. And then, non-treated graphite powder (G), HG or AG was milled with Li to synthesize lithium-graphite intercalation compounds, which are denoted as Li-G, Li-HG and Li-AG, respectively. In XRD profiles of Li-G and Li-HG, it was revealed that the peaks correspond to LiC6 and LiCl2, while no peaks were observed in thedoi:10.7209/tanso.2008.136 fatcat:lxtdmbyfvvgg7orwoafe3cvhaa