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Two poly(benzyl ether) dendrons, decorated in their periphery with nitrile groups, were divergently synthesized and fully characterized. Their gelation properties were studied by using scanning electron microscopy (SEM), X-ray crystal structure analysis and concentration-and temperature-dependent 1 H NMR spectroscopy. It was found that the gelation capability of these dendrons was highly dependent on dendron generation, and the second-generation dendron G 2 -CN proved to be highly efficientdoi:10.1007/s11434-012-5479-2 fatcat:dvf5ghbnrzem3jf5x7q53acw3m