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Synthesis and characterization of pyrazoline derivatives obtained from 4-bromo-naphthalen-1-ol
2015
Scholars Research Library Der Pharma Chemica
unpublished
were cyclized with nucleophiles like phenyl hydrazine / semicarbazide / thiosemi carbazide in DMF solvent and refluxed for 2 hours. The cooled reaction mixture was diluted with water the semisolid so obtained was triturated with ethanol to get a solid which was recrystallised from ethanol-acetic acid mixture to get pyrazoline derivatives. The synthesized compounds were characterized by elemental analysis, 1H NMR, IR Spectroscopy.
fatcat:72altbpy6bb33mbbdcynmenxbm