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In this paper, we report the results obtained from different phases of metal hydrides. The synthesis and characterization of tantalum hydrides were obtained "in situ" during mechanical milling. Elemental Ta with purity of 99.8% was used in this investigation to obtain the hydrides. A highenergy ball milling technique was utilized to prepare hydrogenated phases. Ta hydrides and oxides were formed as function of milling process time. Milling times of 5, 10 and 20 hours were programmed, and thedoi:10.4236/anp.2014.34020 fatcat:ae62t3tqyzdghcew2hhx7bzofm