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C8H10N2O2, monoclinic, P12i/cl (no. 14), a = 12.456(3) Â, b = 5.008(1) Â, c = 13.681(4) k,ß = 96.017(4)°, V= 848.7 Â 3 , Z = 4, Rgt(F) = 0.057, wRreiF 2 ) = 0.166, T= 296 K. Source of material The title compound was synthesized by reaction of hydroxyurea (0.026 mol) with benzyl chloride (0.034 mol) in methanol (100 ml) in the presence of potassium hydroxide (0.034 mol). After refluxing for 13 h, the solution was distilled in the reduced pressure at 35 °C. The resulting crude solid was filtereddoi:10.1524/ncrs.2009.0238 fatcat:rhjokcgvr5brjji3qbo6lcdwci