& mmm NUCLEAR TECHNOLOGY-CHEMISTRY AND CHEMICAL ENGINEERING (M -5 6 7 9 , 2 6 t h Ed.) T h is d o c u m e n t c o n s i s t s o f 1 7 P a g e s , N u m b e x L 9 8 _ o f 2j?7 C o p i e s , S e r i e s A FORMATION O F HYDRAZOIC ACID FROM HYDRAZINE IN N ITRIC ACID SOLUTIONS by E. K enneth Dukes and R ic h a rd M. W a lla ce S e p te m b e r 1962 by i f f t l ' x ' ~ / 7 t . by atetty «LA ■> l i iwsml a»ti -J j & 3 R E^R IC T E D DATA T h is d o c u m p^v^S n ta ln s R e s tr jj^x S^f e a ta as d

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... f in e d A tom ic E n e p^j « P o f 1954. I t s t j r t o y & z t a l o r th e d l^f^S s u r e o f I t s c o n t e b^^. n any m an n er Apy'an u n a u th o r iz e d p e r s o n I s p r o h i b i t e d . Ê . I . du P o n t de Nemours 4 Co. E x p lo s iv e s D ep artm en t -Atomic E n erg y D iv is io n T e c h n ic a l D iv is io n -Savannah R iv e r L a b o r a to r y A ik en , S o u th C a r o lin a C o n tra c t A T (0 7 -2 )-l w ith th e U n ite d S t a t e s A tom ic Energy C om m ission Approved by C. H. I c e , R e s e a rc h Manager S e p a r a tio n s C h e m is try D iv is io n UNCLASSIFIED ABSTRACT A study was made of the kinetics and stoichiometry of the formation of hydrazolc acid In nitric acid solutions containing hydrazine and ferrous sulfamate. The data were used to establish safe limits for the use of hydrazine in process solutions.