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Eisen(III)phthaloeyanine: Darstellung und spektroskopische Charakterisierung von [Fe(OR)2Pc(—2)]- (R = H, CH3, C2H5, (CH3)2CH, (CH3)3C), (FePc(—2))2O und FeXPc(—2) (X = F, Cl, Br, I)/ Iron(III)phthalocyanines: Preparation and Spectroscopic Characterisation of [Fe(OR)2Pc(—2)]- (R = H, CH3, C2H5, (CH3)2CH, (CH3)3C), FePc(—2))2O and FeXPc(—2) (X = F, Cl, Br, I)
1983
Zeitschrift für Naturforschung. B, A journal of chemical sciences
The preparation of bis-hydroxophthalocyaninatoferrate(III) and of some of the bis-alkoxo-analogues is described. In the presence of a small excess of OR -(R = H, CH3, C2H5, (CH3)2CH, (CH3)3C) these complexes are stable in most common non-polar solvents and can be isolated as analytically pure bis-triphenylphosphiniminium-(PNP)-salts. Solutions of these complexes react immediately with water and acids. Thus hydrolysis is an easy way to prepare μ-oxo-bis-phthalocyaninatoiron(III). The reaction
doi:10.1515/znb-1983-0414
fatcat:64flidc5tbbw7fvexqjnk4b5my