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Au nanoparticles (AuNPs) were prepared by reducing HAuCl4 with NaBH4, and then adsorbed uniformly on the surface of carboxylated nanocrystalline cellulose (CNCC). The obtained AuNPs/CNCC particles were doped into a conductive polymer of poly(3,4-ethylenedioxythiophene) (PEDOT) to yield a highly conductive nanocomposite, which was deposited onto a glassy carbon electrode (GCE) by an electrochemical method. The PEDOT/AuNPs/CNCC nanocomposite showed low electrochemical impedance and gooddoi:10.21967/jbb.v3i1.142 fatcat:cwr4kvtsv5g2fltyux4ckil4rq