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Crystal Structure and Phase Transition of 4-Aminopyridinium Tetrabromoantimonate(III) as Studied by Bromine and Antimony NQR, Proton NMR, and Single Crystal X-Ray Diffraction

Masao Hashimoto, Shinichi Hashimoto, Hiromitsu Terao, Masayuki Kuma, Haruo Niki, Hiroyuki Ino
2000 Zeitschrift fur Naturforschung A-A Journal of Physical Sciences  

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The crystal structure of the room temperature phase (RTP) of the title compound was determined at 297 K (monoclinic, space group C2/c, a = 1384.2(2), b = 1377.8(3), c = 755.5(2) pm, β = 121.58(1)°). A complicated disorder was found for the cation. A phase transition from the low-temperature phase (LTP) to the RTP was found at (224 ±1) K (T
doi:10.1515/zna-2000-1-229 fatcat:5h2g6td3hzas5a2hfsdub6q7oe
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Masao Hashimoto, Shinichi Hashimoto, Hiromitsu Terao, Masayuki Kuma, Haruo Niki, Hiroyuki Ino. "Crystal Structure and Phase Transition of 4-Aminopyridinium Tetrabromoantimonate(III) as Studied by Bromine and Antimony NQR, Proton NMR, and Single Crystal X-Ray Diffraction." Zeitschrift fur Naturforschung A-A Journal of Physical Sciences 55.1-2 (2000)