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Crystal structure of methyl 2-(2-formyl-3,4,5-trimethoxyphenyl)acetate, C13H16O6
2006
Zeitschrift für Kristallographie - New Crystal Structures
CnHieOe, triclinic, PI (no. 2), a = 7.343(2) Ä, b = 8.972(2) Ä, c = 10.152(2) A,a = 81.12(2) 0 , β = 77.997(2)°, γ = 80.22(2)°, V = 639.8 Ä 3 , Ζ = 2, R & (F) = 0.081, wR^F 2 ) = 0.239, Τ = 191 Κ. Source of material Phosphorus oxychloride (5.3 g, 0.034 mol) was added drop wise to a stirred solution of methyl 3,4,5-trimethoxyphenylacetate (7 g, 0.029 mol) in freshly distilled ATJV-dimethylformamide (30 ml) at 550 °C. The solution was then heated at 100 °C for 10 minutes and stirred overnight.
doi:10.1524/ncrs.2006.221.14.497
fatcat:pglq2bgds5ggpd453ez3opd2cq