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Synthesis and spectral characterization of Nin, Cull and znii complexes of trioxadiazamacrocycles derived from 1, 13-diamino-4, 7,1 0-trioxatridecane and benzil or 4,4' -dimethylbenzil

R. N. Prasad, Priyanka Sharma
2011 Zenodo  

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Department of Chemistry, University of Rajasthan, Jaipur-302 055, Rajasthan, India E-mail: rnp_l949@yahoo.co.in Manuscript received 10 June 2010. revised 14 January 2011, accepted 02 February 2011 1 + 1 Cyclocondensation of a-diketones such as benzil, 4,4' -dimethylbenzil with I ,13-diamino-4, 7,10- trioxatridecane in the presence of NiII , CuII and znII as templates has yielded complexes of the type [NiLCI]CI, [CuL(NO3)](NO3) and [ZnLCI2) (where L = 17-membered N203 macrocycle). These
more » ... have been characterized by elemental analyses, molar conductances, FAB mass, IR, electronic and 1H NMR spectra.
doi:10.5281/zenodo.5790397 fatcat:njjni2zwprdyradr5umfn77wvm
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R. N. Prasad, Priyanka Sharma. "Synthesis and spectral characterization of Nin, Cull and znii complexes of trioxadiazamacrocycles derived from 1, 13-diamino-4, 7,1 0-trioxatridecane and benzil or 4,4' -dimethylbenzil." Zenodo (2011)