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In this study, the spinel-type ZnMn2O4 material was successfully synthesized via hydrothermal method. Several factors influencing the synthesis of material such as Zn/Mn mole ratio, hydrothermal temperature and calcination temperature were studied. The characterization of expected samples using X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier Transform Infrared (FTIR), surface area analysis (BET) was conducted. The XRD results indicated that the highly ordered crystallinedoi:10.51316/jca.2020.050 fatcat:77hga2beizdp7jyfqetdweagdu