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Dispersion of TiO 2 on montmorillonite pillared aluminium has been done successfully. The photocatalyst were prepared by intercalation of Al 13 onto natural montmorillonite and then calcined at 500 o C. Titania dispersion onto aluminium pillared montmorillonite was carried out by impregnation method at the theoritic concentration of 0.4, 0.8, 1 and 3% titania. The photocatalyst then characterized by XRD, porosimetry, SEM and Diffuse Reflectance Visible methods. Results of characterizationdoi:10.20885/eksakta.vol13.iss1-2.art3 fatcat:p23ykt4vhvg73fwtj4sp65mwwy