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Direct laser writing is an effective technique for fabrication of complex polymeric 3D polymer networks using ultrashort laser pulses. Practically, it remains a challenge to design and fabricate high performance materials with different functions that possess a combination of high strength, substantial ductility, and tailored functionality, in particular for small feature sizes. To date, it is difficult to obtain a time-resolved microscopic picture of the printing process in operando. To closedoi:10.21203/rs.3.rs-151096/v1 fatcat:iulkvlybgbdjnbhsub5wtwnrue