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In this paper, a hydrothermal synthesis method was applied to load Ni-Co Layered Double Hydroxide (LDH) directly on the Nickel foam (NF) as precursor, and by using an electrodeposition method to gain the Co(OH)2/Ni-Co LDH composite. The structure and morphology of as-obtained composite was characterized by X-ray diffractometer (XRD) and scanning electron microscopy (SEM). Electrochemical performances of the as-obtained composite were tested by cyclic voltammetry and galvanostaticdoi:10.20964/2019.06.06 fatcat:6hikon5snbc37pwnrhgowmo45u