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An HPLC method for digoxin quantification in dissolution samples obtained as per the official British Pharmacopeia (BP) method is presented in this paper. The chromatography was performed at 20 °C on a Symmetry C18; 3.5 μm, 75 mm×4.6 mm column with water-acetonitrile (72:28, v/v), as the mobile phase and UV detection at 220 nm. The method was found to be selective, linear, accurate and precise in the specified ranges. The LOD and LOQ were 0.015 and 0.050 µg mL -1 , respectively. Robustnessdoi:10.2298/jsc100106123m fatcat:pc7k5lbeyrdnxnigj3ei6wvdcy