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An environmentally compatible and size-controlled method has been employed for synthesis of superparamagnetic magnetite nanoparticles with prehydrolysate from corn stover. Various characterizations involving X-ray diffraction (XRD), standard and high-resolution transmission electron microscopy (TEM and HRTEM), selected area electron diffraction (SAED), and thermogravimetric analysis (TGA) have integrally confirmed the formation of magnetite nanoparticles with homogeneous morphology and thedoi:10.15376/biores.9.1.589-601 fatcat:u5nos6zgzrgwbnq3uub7knacbq