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2-6-3 Crystal structure analysis of TBAC semiclathrate hydrate by powder diffraction
2-6-3 TBACセミクラスレートハイドレートの粉末回折による結晶構造解析
Proceedings of the Annual Conference of The Japan Institute of Energy
2-6-3 TBACセミクラスレートハイドレートの粉末回折による結晶構造解析
Preserved Fulltext
The crystal structure of tetra-n-butylammonium chloride (TABC) semiclathrate hydrate is affected by the synthesis condition (especially concentration of the TBAC solutions). Two samples of TBAC semiclathrate hydrate and methane TBAC semiclathrate hydrate, essentially having tetragonal structure-I (TS-I), were prepared. The temperature dependence of powder diffraction patterns for these samples revealed growth of unknown peaks above 263 K. These unknown peaks indicate a different from TS-I.
doi:10.20550/jietaikaiyoushi.27.0_66
fatcat:e43wrmw7x5gdjl6jdbbbcpheqe