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N,N,N',N'-tetrakis-(2-benzimidazolylmethyl)-1,2-ethanediamine (TBIMEDA), was prepared by reaction of ethylenediamine tetra-acetic acid disodium salt (EDTA) with 1,2-diaminobenzene in a refluxed glycol solution, and furthermore, three allomeric complexes [(M II TBIMEDA) SO 4 ·5H 2 O, M = Cd, Co, Ni] were selfassembled by solvothermal method based on reaction of this ligand with the relative sulfates respectively. These allomeric complexes were characterized by elemental analysis and IRdoi:10.4236/ojic.2012.24011 fatcat:6m7gtratfrclzpslnqz7mkttfq