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In this work, TiO 2 powders were prepared by high energy vibrating ball milling. X-ray diffraction (XRD), Scanning electron microscopy (SEM) and Photon cross correlation spectroscopy (PCCS with Nanophox) were used to determine the crystallite size of anatase TiO 2 . Depending on the grinding conditions (short grinding time, ball diameter, stainless steel ball and grinding powder ratio), the crystallite size decreased from 34 nm to 8 nm. The average diameter of a TiO 2 particle with 8 nmdoi:10.4236/msce.2021.911002 fatcat:reenoi5qlbd2lok7mda3nphyye