(E)-N-(1,3-Oxazolidin-2-ylidene)benzamide

Hong-Gang An
2007 Acta Crystallographica Section E  
Key indicators: single-crystal X-ray study; T = 293 K; mean (C-C) = 0.003 Å; R factor = 0.045; wR factor = 0.122; data-to-parameter ratio = 14.5. The aryl and oxazolidine rings in the title compound, C 10 H 10 N 2 O 2 , are essentially coplanar [dihedral angle = 3.8 (6) ]. The crystal structure involves intra-and intermolecular N-HÁ Á ÁO hydrogen bonds. Related literature For related literature, see: Allen (2002); Jiang et al. (2006); Lorente et al. (1995); Zhang et al. (2003). Experimental
more » ... ). Experimental Crystal data C 10 H 10 N 2 O 2 M r = 190.20 Orthorhombic, Pccn a = 11.4194 (18) Å b = 20.590 (3) Å c = 8.0325 (13) Å V = 1888.7 (5) Å 3 Z = 8 Mo K radiation = 0.10 mm À1 T = 293 (2) K 0.25 Â 0.23 Â 0.18 mm Data collection Bruker SMART APEX CCD areadetector diffractometer Absorption correction: multi-scan (SADABS; Bruker, 2000) T min = 0.973, T max = 0.988 9475 measured reflections 1850 independent reflections 1091 reflections with I > 2(I) R int = 0.095
doi:10.1107/s1600536807030772 fatcat:7clrhnm5zfahrovbhth7khussq