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Developed and validated for the determination of Atorvastatin (ATV) and Bezafibrate (BZF) in the tablets dosage forms using spectrophotometric and Spectrofluorimetric methods. The spectrophotometric methods were based on derivatization of the investigated drugs with two reagents NQS and NBD-Cl. Beer's law was obeyed over the ranges of 0.3 - 6 and 0.5- 9 µg/mL for NQS reaction, and the ranges of 0.5 - 5 and 1-10 µg/mL for NBD-Cl reaction, the absorbance readings of ATV and BZF, respectively.doi:10.5281/zenodo.2567534 fatcat:qivgg6td6bay5na6aou7eogruu