Crystal structure of (E)-1-(4-(((E)-5-bromo-2-hydroxybenzylidene)amino)phenyl)ethan-1-one O-methyl oxime, C16H15BrN2O2

Ji-Xing Zhao, Li Zhao, Peng-Peng Li, Fei Wang, Qin-Qin An
2017 Zeitschrift für Kristallographie - New Crystal Structures  
C 16 H15BrN 2 O 2 , monoclinic, P21/c (no. 14), a = 33.758(5) Å, b = 7.1117(16) Å, c = 6.2194(9) Å, β = 92.133 (13) CCDC no.: 1564491 The structure is shown in the figure. Tables 1 and 2 contain details on crystal structure and measurement conditions and a list of the atoms including atomic coordinates and displacement parameters. Source of material All chemicals were used without further purification. 4-amino acetophenone methoxy oxime was prepared by a method reported earlier [1] [2] [3] . To
more » ... er [1] [2] [3] . To an ethanol solution (5 mL) of 5bromosalicylic acid (201.0 mg, 1 mmol) was added an ethanol solution (5 mL) of 4-aminoacetophenone methoxy oxime (164.0 mg, 1 mmol). The solution was stirred at 328 K for 12 h. The residue was washed with ethanol and hexane, then place in the drying oven for 2 days to get a light brown powder (yield
doi:10.1515/ncrs-2016-0407 fatcat:bmwqg2hkjjed5ci5hbdmdczzk4