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Preparation of pure three-dimensional graphene (3DG) with high rate performance for supercapacitors is critical for fast rate charge/discharge. Here, 3DG was prepared via thermal annealing of freeze-dried reduced graphene oxide (RGO) hydrogel under inert gas protection. The formed 3DG as an electrode material for supercapacitors revealed a specific capacitance of 115 F·g−1 at a current density of 1 A·g−1, and a high capacitance retention of 70% as current density increased to 40 A·g−1. Thedoi:10.3390/app9112188 fatcat:5gtfwtaqhba2lisgznz52xqnti