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Nickel nanoparticles were synthesized by the chemical reduction of NiCl2 with N2H4 under controlled pH environment. During nucleation, polyvinyl pyrrolidone (PVP) was added as the protective agents for preventing the agglomeration of metal clusters. Color of the solution changed from green to blue during the reaction period. X-Ray Adsorption Spectroscopy (XAS), X-Ray Diffraction (XRD), and Transmission Electron Microscopy (TEM) analytical methods were used to characterize the product. XASdoi:10.5755/j01.ms.22.2.12921 fatcat:3igse4jk4vftzjbptshy4ybjaa