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<p>Pyrolysis gas chromatography mass spectrometry (Py-GC/MS) studies were carried out on the Nigerian and US corn stalks at 500 °C. Analyses of the fast pyrolysis products showed that the Nigerian corn stalks produced more diverse compounds like: acetaldehyde, acetic acid methyl ester, 2,3-pentanedione, 1-hydroxy-2-butanone, butanedial, phenol and vanillin. On the other hand, the pyrolyzed US corn stalks produced compounds like: furfural, phenol, 2-methoxy, 2-methylbenzaldehyde, anddoi:10.14419/ijac.v3i1.4328 fatcat:v7jlipfonvc7ddfe7jjeqyj2z4