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Cu 6 (P 1-x As x )S 5 I mixed crystals were grown using chemical vapour transport. Temperature isoabsorption investigations of optical absorption edge enable to reveal anomalies typical for the first-and second-order phase transitions as well as to construct the x, T-diagram. The spectrometric measurements of the optical absorption edge in S As P Cu 5 x x 1 6 superionic mixed crystals have been studied.doi:10.15407/spqeo16.02.146 fatcat:3mq7v5p34zav5hk4eddaqsct7i