Crystal structure of dichloridobis{μ2-2,2′-((1E,1′E)-(ethane-1,2-diylbis(azanylylidene))bis(methanylylidene))bis(4-chlorophenolato)-κ5O,N,N′,O′:O′}diiron(III), C32H24Cl6Fe2N4O4

Mauricio Fuentealba, Deborah González, Vania Artigas
2016 Zeitschrift für Kristallographie - New Crystal Structures  
C 32 H 24 Cl 6 Fe 2 N4O4, triclinic, P¯ (No. 2), a = 7.3325(10) Å, b = 9.1317(14) Å, c = 13.161(2) Å, α = 105.927(4)°, β = 95.407(4)°, γ = 96.752(4)°, V = 834.1(2) Å 3 , Z = 1, Rgt(F) = 0.0382, wR ref (F 2 ) = 0.0897, T = 296.15 K. CCDC no.: 1483817 The crystal structure is shown in the gure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material Methanol was dried and distilled according to
more » ... lled according to standard procedures. 5-Chlorosalicylaldehyde, ethylendiamine and iron(II) chloride tetrahydrate were purchased from Aldrich and used without further puri cation. Crystals were
doi:10.1515/ncrs-2016-0081 fatcat:htqfozqhqbevdl7b4hvhiqt65e