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Recebido em 2/2//06; aceito em 25/4/06; publicado na web em 30/8/06 SULFADIMETHOXYNE QUANTIFICATION IN MILK BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY. A method for HPLC determination of sulfadimethoxyne in milk is presented. The analyte isolation and concentration were performed by solidphase extraction through a C-8 cartridge, pre-conditioned with hexane, methanol and water and eluted with MeOH. The recovery determination was done with a spiked solution of 20, 50 or 100 μg L -1 . In thisdoi:10.1590/s0100-40422007000100018 fatcat:ymq3aplh55dnzbiztwburkhtye