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An unprecedented molecular 2Fe-2As precursor complex was synthesized and transformed under soft reaction conditions to produce an active and long-term stable nanocrystalline FeAs material for electrocatalytic water oxidation in alkaline media. The 2Fe2As-centred beta-diketiminato complex, having an unusual planar Fe2As2 core structure, results from the salt-metathesis reaction of the corresponding beta-diketiminato (FeCl)-Cl-II complex and the AsCO- (arsaethynolate) anion as the monoanionic As-doi:10.17169/refubium-28782 fatcat:uccqqwx6vrhtdaeefbyxv47vq4