Crystal structure of (Z)-3-hydroxy-3-(4-methoxyphenyl)-1-(pyridin-2-yl)prop-2-en-1-one, C15H13NO3

Smaail Radi, Said Tighadouini, Driss Eddike, Yahia N. Mabkhot, Monique Tillard
2017 Zeitschrift für Kristallographie - New Crystal Structures  
C15H 13 NO 3 , monoclinic, Cc (No. 9), a = 3.9230(3) Å, b = 26.578(2) Å, c = 11.7147(12) Å, β = 94.028(8)°, V = 1218.4(2) Å 3 , Z = 4, Rgt(F) = 0.0387, wR ref (F 2 ) = 0.0877, T = 173 K. CCDC no.: 1525410 The asymmetric unit of the title crystal structure is shown in the gure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material To a suspension of sodium (0.4 g; 17.40 mmol) in anhydrous
more » ... ) in anhydrous toluene, was added ethyl 2-picolinate (2 g; 13.28 mmol) in toluene. Then 1-(4-methoxphenyl) ethanone (1.99 g;
doi:10.1515/ncrs-2016-0219 fatcat:cmeyjwso3zce3kys4xhrufgxpu