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A simultaneous separation process of two anticancer drugs carboplatin and temozolamide in their binary mixture using capillary zone electrophoresis method has been introduced in this study. Under full optimized conditions a fused silica capillary was used to carry out the electrophoretic separation using a background electrolyte 50 mmol L -1 acetate buffer of pH = 3.6 which was run at potential 20 kV, hydrodynamic injection 8 s and 60 mbar pressure. The capillary cartridge temperature wasdoi:10.20964/2018.05.55 fatcat:ljcsiqzx7vbj3bxzhemvfscyga