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C 20H20CuN2O5, monoclinic, P121/c1 (no. 14), Source of material An aqueous mixture (8 ml) of Cu(CH 3COO)2 · H2O (0.0394 g, 0.2 mmol), H 2chdc (0.0346 g, 0.2 mmol), 1,10-phenanthroline (0.0403 g, 0.2 mmol), and NaOH (0.0117 g, 0.3 mmol) in a molar ratio of 1:1:1:1.5 was placed in a teflon-lined stainless vessel, which was sealed and placed in an oven at 170°C for 5 h. Blue column-like crystals were obtained after the mixture was cooled to room temperature.doi:10.1524/ncrs.2004.219.1.63 fatcat:gw6c4eoptzallmk3ivrlylcjt4