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Slow evaporation of a dilute DMSO solution of the title compound at room temperature, provided a brown crystal of Ni(CMTSC)2DMSO suitable for X-Rays study (space group: P-1, a(Å)=8.1750 (3) (5) ). Two Ni atoms were located on special positions providing two molecules of Ni(CMTSC)2 different for their torsion angles and intermolecular interactions. In both molecules, the thiosemicarbazone coordinates as an anionic ligand via the thiosemicarbazone moiety's azomethine nitrogen and thiolatosulphurdoi:10.13171/mjc.4.5.2015.18.11.23/boukli fatcat:g3v3345yejchrdm7bkzrtjyeoa