Crystal structure of (E)-2-(((1,10-phenanthrolin-5-yl)imino)methyl)-5-methylphenol monohydrate, C20H15N3O·H2O

Mampotso S. Tsosane, Hendrik G. Visser, Alice Brink
2016 Zeitschrift für Kristallographie - New Crystal Structures  
C 20 H15N 3 O·H 2 O, triclinic, P¯ (No. 2), a = 7.066(3) Å, b = 9.996(4) Å, c = 12.873(5) Å, α = 86.007(14)°, β = 74.861(14)°, γ = 69.596(13)°, V = 822.4(6) Å 3 , Z = 2, Rgt(F) = 0.0424, wR ref (F 2 ) = 0.1241, T = 100 K. CCDC no.: 1442787 The crystal structure is shown in the gure, Tables 1-3 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material The title compound was synthesized according to the
more » ... ng to the literature procedures [1, 2] using 1,10-phenanthrolin-5-amine (0.359 g, 1.84 mmol) and 2-hydroxy-4-methylbenzaldehyde (0.254 g, 1.87 mmol) in methanol. The product was obtained as an orange powder which was washed with cold methanol
doi:10.1515/ncrs-2015-0103 fatcat:a5bl7vxf2nby7phqqvs42qrtje