Crystal structure of 1,1-dimethyl-3-(4-methoxyphenyl)urea, C10H14N2O2

Gamal A. El-Hiti, Keith Smith, Mohammed B. Alshammari, Amany S. Hegazy, Benson M. Kariuki
2017 Zeitschrift für Kristallographie - New Crystal Structures  
C 10 H14N 2 O 2 , monoclinic, P21/c (no. 14), a = 14.9185(12) Å, b = 7.7243(6) Å, c = 9.2229(5) Å, β = 91.032(6)°, V = 1062.63(13) Å 3 , Z = 4, T = 293(2) K. CCDC no.: 1525571 The asymmetric unit of the title crystal structure is shown in the figure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material To a stirred solution of triphosgene (1.0 mole equivalent) in dichloromethane (DCM), a
more » ... ethane (DCM), a solution of 4-methoxyaniline (2.5 mole equivalents) and triethylamine (5.5 mole equiva-
doi:10.1515/ncrs-2016-0238 fatcat:2mrlr62kvjge5mqqxd76scex3q