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A ligand-and CO gas-free condition is developed in palladium-catalyzed three-component reaction of iodoanilines, unsaturated compounds and Mo(CO) 6 as a solid carbon monoxide source. The approach allows for smooth construction of biologically interesting 3,4-disubstituted (dihydro)quinolin-2(1H)-ones in presence of catalytic amounts of palladium and avoids the problematic use of gaseous carbon monoxide.doi:10.3998/ark.5550190.p008.531 fatcat:ebdtcc6ab5emnix4s3soug5p5i