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Topotactic transformation was one of the most frequently related processes in the synthesis process of cobalt oxide nanomaterials. Microstructural evolution studies of this process inform and enable the process of controlling the shape of the final products. One such topotactic transformation was investigated here, the transition from Co(OH)2 hexagonal nano platelets to Co3O4 octahedra by a hydrothermal method in an ammonia solution. Evolution of phase and microstructure was studied duringdoi:10.5755/j01.ms.25.3.22005 fatcat:i6vrakxpiba2jmob2l32tr6dki