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In this paper, CeVO 4 /FeVO 4 nanocomposites were prepared by direct feeding microwave synthesis method with nine water iron nitrate (Fe(NO 3 ) 3 •9H 2 O), cerium nitrate hexahydrate (Ce(NO 3 ) 3 •6H 2 O) and ammonium metavanadate (NH 4 VO 3 ) as raw material and Sodium Dodecyl Sulfate (SDS) as surfactant. Then X-Ray Diffractometer (XRD) and Scanning Electron Microscopy (SEM) were used to observe the CeVO 4 /FeVO 4 nanocomposites. SEM image showed that the as-prepared CeVO 4 / FeVO 4doi:10.4236/msce.2016.45004 fatcat:oas32aizgvanzgqg3olw3mivtu