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This work describes the synthesis of CuBi2O4 material which, as reported in a literature work, presents photoactivity, behaving as a p-type material, having the ability to cleave the water molecule and reduce H + ions in hydrogen gas (H2 (g)). ), considered a renewable fuel source. The synthesis was done by the pyrolysis spray process, using an airbrush, a method that makes it possible to obtain thin and homogeneous films and then heat treatment, with different heating steps in one sample, anddoi:10.33448/rsd-v9i2.2021 fatcat:5eq53p2q5bhspiguwvseogwzcm