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C 7 H 6 ClNO 2 ,orthorhombic, P2 1 2 1 2 1 (no. 19), a =4.745 (2) Source of material Thec ompoundw as obtained upon photodecarboxylation of 4nitro-phenylacetic acid in thepresence of tert-butylhypochlorite and iodine according to apublished procedure . Experimental details Carbon-boundHatoms were placed in calculated positions with d(C-H)=0.99Åfor themethylene groupand d(C-H)=0.95Å foraromaticcarbonatoms andwereincludedinthe refinement in the riding model approximation with U(H) =1 .2 U eqdoi:10.1524/ncrs.2011.0261 fatcat:kcspoktwvjcg7kdtesbvkqctxy