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Crystal structure of [chlorobis(1,10-phenanthroline)copper(II)] chloride 3,5-dihydroxybenzoic acid solvate monohydrate, [CuCl(C12H8N2)2]Cl · C6H3(OH)2COOH · H2O
2005
Zeitschrift für Kristallographie - New Crystal Structures
C31H24CI2CUN4O5, monoclinic, P\2\ln\ (no. 14), a = 15.380(3) A, b = 11.466(2) A, c = 17.150(3) A, β = 109.99(3)°, V = 2842.2 A 3 , Ζ = 4, R#(F) = 0.066, yvRniF 1 ) = 0.197, T= 295 K. Source of material A mixture of CuCh · 2H 2 0 (0.0524 g, 0.31 mmol), 3,5-dihydroxybenzoic acid (0.0917 g, 0.60 mmol), 1,10-phenanthroline (0.1214 g, 0.61 mmol) and water (10 ml) was heated at 393 Κ for 24 h in a 20 ml Teflon-lined stainless-steel autoclave. After cooling, a green solution was obtained. The
doi:10.1524/ncrs.2005.220.3.448
fatcat:koe2fa7myvhebbcxij56s4mblm