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C9H19NO8P2, orthorhombic, Pca2\ (no. 29), a = 24.348(4) Ä, b = 8.088(2) Ä, c = 7.623(4) Ä, V= 1501.2 Ä 3 , Ζ = 4, Rgt(F) = 0.039, wRKf(F) = 0.049, Τ = 296 Κ. Source of material Crystals of title compound were synthesized by reaction of stirred ethanolic solution of 2-ethyl-6-methylaniline with concentrated phosphoric acid. Then, the obtained solution was evaporated in air for several days at room temperature until formation of prismatic crystals with suitable size for X-ray analysis.doi:10.1524/ncrs.2005.220.14.157 fatcat:dwz4c4brnve4bkdreqb5wggbbu