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The technique of synthesis and purification of trimethyl(phenyl)silane PhSiMe 3 , allowing to obtain the product with high yield. Individuality of the product was confirmed by elemental analysis for C, H, Si. IR, UV and 1H NMR-spectroscopic studies, defined its spectral characteristics. Complex thermal analysis and thermogravimetric defined thermoanalytical behavior effects of PhSiMe 3 in an inert atmosphere. Tensimetric studies have shown that the compound has sufficient volatility and thermaldoi:10.17073/1609-3577-2014-3-199-205 fatcat:rxtxwvavdrfhhc4xxzsn32wzii