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Well-defined homo glycopolymer/montmorillonite (MMT) nanocomposite (gly 1 ) was prepared successfully by the "grafting from" technique from the modified surface of MMT via surface initiated atom transfer radical polymerization (SI-ATRP) of 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose (gly) in the presence of Cu(I)Br/bipyridyl at 90˚C in xylene. Well-defined diblock copolymers (gly 2 , gly 3 , gly 4 and gly 5 ) were also synthesized via the same technique by using comonomers ofdoi:10.4236/ojopm.2012.24012 fatcat:ec3kiemta5ferk6m2uyup6v7ry