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This article presents results of a study on coating of a polymeric substrate catalyst on metallic surface. Stability of coating on metallic surfaces is a proper specification. Sol-gel technology was used to synthesize adhesion promoters of polysilane compounds that act as a mediator. The intermediate layer was coated by synthesized sulfonated polystyrene-divinylbenzene as a catalyst for production of MTBE in catalytic distillation process. Swelling of catalyst and its separation from the metaldoi:10.2298/ciceq100420033h fatcat:rcw4vdmj7rcvzmdqolqh7oipla