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In this work,Cloud point extraction (CPE) methodology as an one green chemistry method is used for extraction, enrichment and determination ofNi (II) and Cu (II) in the somemedicinal plants,by use organic reagent2-[ (6-Methyl-2-Benzothiazolyl)azo]-4-Chloro Phenol (6-MeBTAClP) for formationthe extracted complexes into micelles of Triton X-114 as a mediated extractant at65,70 C0 respectively. The extracted product in densityhigh (cloud point layer )is separated from the aqueous layer bydoi:10.26452/ijrps.v9ispl1.1379 fatcat:hvl2w2dqbjgn7ha7exlfhxarha